Vickers hardness test


The Vickers hardness test was developed in 1921 by Robert L. Smith and George E. Sandland at Vickers Ltd as an alternative to the Brinell method to measure the hardness of materials. The Vickers test is often easier to use than other hardness tests since the required calculations are independent of the size of the indenter, and the indenter can be used for all materials irrespective of hardness. The basic principle, as with all common measures of hardness, is to observe a material's ability to resist plastic deformation from a standard source.
The Vickers test can be used for all metals and has one of the widest scales among hardness tests.
The unit of hardness given by the test is known as the Vickers Pyramid Number or Diamond Pyramid Hardness. The hardness number can be converted into units of pascals, but should not be confused with pressure, which uses the same units. The hardness number is determined by the load over the surface area of the indentation and not the area normal to the force, and is therefore not pressure.

Implementation

It was decided that the indenter shape should be capable of producing geometrically similar impressions, irrespective of size; the impression should have well-defined points of measurement; and the indenter should have high resistance to self-deformation. A diamond in the form of a square-based pyramid satisfied these conditions. It had been established that the ideal size of a Brinell impression was of the ball diameter. As two tangents to the circle at the ends of a chord 3d/8 long intersect at 136°, it was decided to use this as the included angle between plane faces of the indenter tip. This gives an angle from each face normal to the horizontal plane normal of 22° on each side. The angle was varied experimentally and it was found that the hardness value obtained on a homogeneous piece of material remained constant, irrespective of load. Accordingly, loads of various magnitudes are applied to a flat surface, depending on the hardness of the material to be measured. The HV number is then determined by the ratio F/A, where F is the force applied to the diamond in kilograms-force and A is the surface area of the resulting indentation in square millimeters. A can be determined by the formula.
which can be approximated by evaluating the sine term to give,
where d is the average length of the diagonal left by the indenter in millimeters. Hence,
where F is in kgf and d is in millimeters.
The corresponding unit of HV is then kilograms-force per square millimeter or HV number. In the above equation, "F" could be in N and "d" in mm, giving HV in the SI unit of MPa. To calculate Vickers hardness number using SI units one needs to convert the force applied from newtons to kilogram-force by dividing by 9.806 65. This leads to the following equation:
where F is in N and d is in millimeters. A common error is that the above formula to calculate the HV number does not result in a number with the unit Newton per square millimeter, but results directly in the Vickers hardness number, which is in fact kilograms-force per square millimeter.
Vickers hardness numbers are reported as xxxHVyy, e.g. 440HV30, or xxxHVyy/zz if duration of force differs from 10 s to 15 s, e.g. 440HV30/20, where:
To convert the Vickers hardness number to SI units the hardness number in kilograms-force per square millimeter has to be multiplied with the standard gravity to get the hardness in MPa and furthermore divided by 1000 to get the hardness in GPa. Vickers hardness can also be converted to an SI hardness based on the projected area of the indent rather than the surface area. The projected area,, is defined as the following for a Vickers indenter geometry:
This hardness is sometimes referred to as the mean contact area and ideally can be directly compared with other hardness tests also defined using projected area.
Vickers values are generally independent of the test force: they will come out the same for 500 gf and 50 kgf, as long as the force is at least 200 gf.However, lower load indents often display a dependence of hardness on indent depth known as the indentation size effect.
For thin samples indentation depth can be an issue due to substrate effects. As a rule of thumb the sample thickness should be kept greater than 2.5 times the indent diameter. Alternatively indent depth,, can be calculated according to:
MaterialValue
316L stainless steel140HV30
347L stainless steel180HV30
Carbon steel55–120HV5
Iron30–80HV5
Martensite1000HV
Diamond10000HV

Precautions

When doing the hardness tests the minimum distance between indentations and the distance from the indentation to the edge of the specimen must be taken into account to avoid interaction between the work-hardened regions and effects of the edge. These minimum distances are different for ISO 6507-1 and ASTM E384 standards.
StandardDistance between indentationsDistance from the center of the indentation to the edge of the specimen
ISO 6507-1> 3·d for steel and copper alloys and > 6·d for light metals2.5·d for steel and copper alloys and > 3·d for light metals
ASTM E3842.5·d2.5·d

Estimating tensile strength

If HV is first expressed in N/mm2, or otherwise by converting from kgf/mm2, then the tensile strength of the material can be approximated as ≈ HV/ ≈ HV/3, where is a constant determined by yield strength, Poisson's ratio, work-hardening exponent and geometrical factors usually ranging between 2 and 4. In other words, if HV is expressed in N/mm2 then the tensile strength ≈ HV/3. This empirical law depends variably on the work-hardening behavior of the material.

Application

The fin attachment pins and sleeves in the Convair 580 airliner were specified by the aircraft manufacturer to be hardened to a Vickers Hardness specification of 390HV5, the '5' meaning five kiloponds. However, on the aircraft flying Partnair Flight 394 the pins were later found to have been replaced with sub-standard parts, leading to rapid wear and finally loss of the aircraft. On examination, accident investigators found that the sub-standard pins had a hardness value of only some 200-230HV5.